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NMR Assignment of N-(1-adamantyl)-1-pentyl-1H-indazole-3-carboxamide Seized as Herbal Incense for the First Time in Italy

The synthetic cannabinoid, N-(1-adamantyl)-1-pentyl-1H-indazole-3-carboxamide, known also as AKB48 and/or APINACA, has been detected for the first time in herbal incense seized in Italy. Its structural characterization has been performed through gas chromatography-mass spectrometry (GC-MS) and high-resolution nuclear magnetic resonance (NMR) analysis. In order to favor an easier and faster identification of AKB48 in future investigations, NMR assignments in deuterated methanol and chloroform is also reported.
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Editorial Board Members Related to Spice

Mohsen Meydani

Professor
Friedman School of Nutrition Science and Policy
Tufts University
United States

Bill Durham

Professor
Department of Chemistry and Biochemistry
University of Arkansas
United States

Mellar P. Davis

Professor
Case Comprehensive Cancer Center
Case Western Reserve University
United States

Jeffrey E. Lee

Assistant Professor
Laboratory Medicine & Pathobiology
University of Toronto
Canada
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